Synthesis and Electrochemical Characterization of Uniformly-Dispersed High Loading Pt Nanoparticles on Sonochemically-Treated Carbon Nanotubes

Synthesis and Electrochemical Characterization of Uniformly-Dispersed High Loading Pt Nanoparticles on Sonochemically-Treated Carbon Nanotubes - Journal Phys. Chem. B, 108, p.19255-19259, 2004 .

A sonochemical process was developed to treat carbon nanotubes in nitric and sulfuric acids to create surface functional groups for metal nanoparticle deposition. Carbon nanotubes treated in the sonochemical process are shown to lead to the deposition of uniformly dispersed high loading Pt nanoparticles, which have not been achieved with carbon nanotubes treated in reflux processes. Pt nanoparticles of a size less than 5 nm and loading up to 30 wt