Efficient synthesis of small molecule macroarrays: optimization of the macroarray synthesis platform and examination of microwave and conventional heating methods (Record no. 43382)

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control field 20250625124733.0
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Transcribing agency CICY
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Classification number (OCLC) (R) ; Classification number, CALL (RLIN) (NR) B-9123
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Title Efficient synthesis of small molecule macroarrays: optimization of the macroarray synthesis platform and examination of microwave and conventional heating methods
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Volume/sequential designation Tetrahedron, 62(19), p.4715-4727, 2006
520 3# - SUMMARY, ETC.
Summary, etc. We report a method for the efficient construction of small molecule macroarrays using microwave-assisted SPOT-synthesis. Macroarrays of 1,3-diphenylpropenones (chalcones)were synthesized rapidly and in high purity starting from robust,Wang-linker-derivatized planar supports.We have optimized the entire chalcone macroarray construction process and evaluated the efficiency and utility of microwave-assisted reactions in array synthesis. Microwave heating was found to be most beneficial for reactions that require temperatures greater than the boiling points of the solvents. These microwave-assisted conditions permitted straightforward access to macroarrays of 2,4,6-triarylpyridines derived from the original chalcone scaffold.
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Personal name Bowman, M. D.
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Personal name Jacobson, M. M.
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Personal name Pujanauski, B. J.
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Personal name Blackwell, H. E.
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Uniform Resource Identifier <a href="https://drive.google.com/file/d/1iFexGsctdmK02Ryc5Qku9iBp5raZ5C8l/view?usp=drivesdk">https://drive.google.com/file/d/1iFexGsctdmK02Ryc5Qku9iBp5raZ5C8l/view?usp=drivesdk</a>
Public note Para ver el documento ingresa a Google con tu cuenta: @cicy.edu.mx
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  Clasificación local     Ref1 CICY CICY Documento préstamo interbibliotecario 25.06.2025   B-9123 25.06.2025 25.06.2025 Documentos solicitados