The mechanism of electrocatalytic oxidation of formic acid on Pt (100) and Pt (111) in sulphuric acid solution: an emirs study (Record no. 46551)

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Classification number (OCLC) (R) ; Classification number, CALL (RLIN) (NR) B-12342
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245 10 - TITLE STATEMENT
Title The mechanism of electrocatalytic oxidation of formic acid on Pt (100) and Pt (111) in sulphuric acid solution: an emirs study
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Volume/sequential designation J. Electroanal. Chem., 240(1-2), p.147-159, 1988
520 3# - SUMMARY, ETC.
Summary, etc. The oxidation of formic acid at single crystal Pt (111)and Pt (100)electrodes in aqueous sulphuric acid was investigated using in-situ IR spectroscopy. The strongly adsorbed poisoning species, CO,,,, was formed more slowly and to a lesser extent on the (111)surface. Correlation between the voltammetry and the spectra led to the assignment of broad bands near 1750 cm-' to absorption by reactive intermediates, probably (COOH),,,. A detailed reaction scheme consistent with the electrochemical and spectroelectrochemical data and featuring linked, parallel pathways involvmg adsorbed poison and adsorbed reactive intermediate, is presented.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Sun, S.G.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Clavilier, J.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Bewick, A.
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Uniform Resource Identifier <a href="https://drive.google.com/file/d/1thxDhCdUqiHbWjtqP27NWoBCZk1oOAjS/view?usp=drivesdk">https://drive.google.com/file/d/1thxDhCdUqiHbWjtqP27NWoBCZk1oOAjS/view?usp=drivesdk</a>
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