Vacuum liquid chromatographic isolation and characterization of beta-sitosterol from the bark of Sarcocephalus latifolius (Smith Bruce). (Record no. 53515)
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| fixed length control field | 01771nam a2200277Ia 4500 |
| 003 - CONTROL NUMBER IDENTIFIER | |
| control field | MX-MdCICY |
| 005 - DATE AND TIME OF LATEST TRANSACTION | |
| control field | 20250625162429.0 |
| 040 ## - CATALOGING SOURCE | |
| Transcribing agency | CICY |
| 090 ## - LOCALLY ASSIGNED LC-TYPE CALL NUMBER (OCLC); LOCAL CALL NUMBER (RLIN) | |
| Classification number (OCLC) (R) ; Classification number, CALL (RLIN) (NR) | B-19386 |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION | |
| fixed length control field | 250602s9999 xx |||||s2 |||| ||und|d |
| 245 10 - TITLE STATEMENT | |
| Title | Vacuum liquid chromatographic isolation and characterization of beta-sitosterol from the bark of Sarcocephalus latifolius (Smith Bruce). |
| 490 0# - SERIES STATEMENT | |
| Volume/sequential designation | Journal of Chemistry and Chemical Sciences, 5(9), p.480-488, 2015 |
| 520 3# - SUMMARY, ETC. | |
| Summary, etc. | The methanol fraction of the stem bark of Sarcocephalus Latifolius (Smith Bruce)was subjected to vacuum liquid chromatography (VLC)isolation method using an isocratic solvent of petroleum ether: ethyl acetate at a ratio of 1:9 by collecting 20ml each and 45 fractions were collected. Based on their Thin Layer Chromatographic (TLC)analysis, fraction 6, 7, 8 and 9 were combined to give SB-C which was further subjected to VLC and eluted isocratically using petroleum ether: ethyl acetate (1:9)to obtain SB-C-1 to SB-C-8 (8 Fraction). Fraction 5 shows a prominent single yellow spot that was cleaned further by Preparative Thin Layer Chromatography (PTLC)to obtain SB-C1. The structure of the compound was established by spectroscopic studies as well as by comparison with existing data. Based on these SB-C1 was proposed to be _-Sitosterol. |
| 650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM | |
| Topical term or geographic name entry element | SARCOCEPHALUS |
| 650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM | |
| Topical term or geographic name entry element | ISOLATION |
| 650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM | |
| Topical term or geographic name entry element | METHANOL |
| 650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM | |
| Topical term or geographic name entry element | CHROMATOGRAPHY |
| 650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM | |
| Topical term or geographic name entry element | SPECTROSCOPIC |
| 650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM | |
| Topical term or geographic name entry element | _-SITOSTEROL |
| 700 12 - ADDED ENTRY--PERSONAL NAME | |
| Personal name | Yinusa, I. |
| 700 12 - ADDED ENTRY--PERSONAL NAME | |
| Personal name | George, N. I. |
| 700 12 - ADDED ENTRY--PERSONAL NAME | |
| Personal name | Ayo, R. G. |
| 700 12 - ADDED ENTRY--PERSONAL NAME | |
| Personal name | Rufai, Y. |
| 856 40 - ELECTRONIC LOCATION AND ACCESS | |
| Uniform Resource Identifier | <a href="https://drive.google.com/file/d/1Z0iKERIYVrIZ8o-RQFvn3NKd0WBQoASq/view?usp=drivesdk">https://drive.google.com/file/d/1Z0iKERIYVrIZ8o-RQFvn3NKd0WBQoASq/view?usp=drivesdk</a> |
| Public note | Para ver el documento ingresa a Google con tu cuenta: @cicy.edu.mx |
| 942 ## - ADDED ENTRY ELEMENTS (KOHA) | |
| Source of classification or shelving scheme | Clasificación local |
| Koha item type | Documentos solicitados |
| Lost status | Source of classification or shelving scheme | Damaged status | Not for loan | Collection | Home library | Current library | Shelving location | Date acquired | Total checkouts | Full call number | Date last seen | Price effective from | Koha item type |
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| Clasificación local | Ref1 | CICY | CICY | Documento préstamo interbibliotecario | 25.06.2025 | B-19386 | 25.06.2025 | 25.06.2025 | Documentos solicitados |