Sensitive determination of auxins in environmental water and peach beverage by hyper crosslinked polymer-based solid-phase extraction with high performance liquid chromatography-fluorescence detection (Record no. 53592)

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fixed length control field 02579nam a2200301Ia 4500
003 - CONTROL NUMBER IDENTIFIER
control field MX-MdCICY
005 - DATE AND TIME OF LATEST TRANSACTION
control field 20250625162431.0
040 ## - CATALOGING SOURCE
Transcribing agency CICY
090 ## - LOCALLY ASSIGNED LC-TYPE CALL NUMBER (OCLC); LOCAL CALL NUMBER (RLIN)
Classification number (OCLC) (R) ; Classification number, CALL (RLIN) (NR) B-19465
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245 10 - TITLE STATEMENT
Title Sensitive determination of auxins in environmental water and peach beverage by hyper crosslinked polymer-based solid-phase extraction with high performance liquid chromatography-fluorescence detection
490 0# - SERIES STATEMENT
Volume/sequential designation Journal of Chromatography A, 1678, p.463345, 2022
520 3# - SUMMARY, ETC.
Summary, etc. As plant regulators, auxins can promote plant growth. However, they have toxicity and may cause harm to humans. Due to their low concentrations in food sample matrices, the enrichment and analysis of trace auxins in food samples is a challenging work. In this work, a series of hyper crosslinked polymers (HCPs)were synthesized by Friedel-Crafts acylation to extract four auxins (indole-3-acetic acid, indole-3-propionic acid, indole-3-butyric acid and 1-naphthylacetic acid). Among these HCPs, the QP-TC-HCP, synthesized from p-quaterphenyl (QP)and terephthaloyl chloride (TC), showed the best adsorption performance for the auxins. It was then applied as the adsorbent for the solid-phase extraction of the auxins from environmental water and peach beverage samples, followed by high performance liquid chromatography-fluorescence detection. Under the optimized conditions, the limits of detection were 3.0-12.0 pg mL-¹ for environmental water and 18.0-36.0 pg mL-¹ for peach beverage sample. The method recoveries of the auxins for the spiked samples were in the range of 85.0-110.0 percent. The established method provided an alternative approach for the determination of auxins in food samples. In addition, different types of organic compounds were tested for the extraction by the QP-TC-HCP to assess its application potential and adsorption mechanism. It was concluded that the QP-TC-HCP had better extraction performance for the compounds with certain hydrophilicity and more hydrogen bonding sites.
650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element AUXINS
650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element HYPER CROSSLINKED POLYMERS
650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element HIGH PERFORMANCE LIQUID CHROMATOGRAPHY
650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element SOLID-PHASE EXTRACTION
650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element FRIEDEL-CRAFTS ACYLATION
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Liu, Z.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Wang, J.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Guo, Y.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Liu, W.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Yang, X.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Wu, Q.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Wang, Z.
856 40 - ELECTRONIC LOCATION AND ACCESS
Uniform Resource Identifier <a href="https://drive.google.com/file/d/1opU_nyyc2gOIwWIVbn6bWePIwafu3_6w/view?usp=drivesdk">https://drive.google.com/file/d/1opU_nyyc2gOIwWIVbn6bWePIwafu3_6w/view?usp=drivesdk</a>
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Source of classification or shelving scheme Clasificación local
Koha item type Documentos solicitados
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  Clasificación local     Ref1 CICY CICY Documento préstamo interbibliotecario 25.06.2025   B-19465 25.06.2025 25.06.2025 Documentos solicitados