MARC details
| 000 -LEADER |
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| fixed length control field |
02265nam a2200301Ia 4500 |
| 003 - CONTROL NUMBER IDENTIFIER |
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| control field |
MX-MdCICY |
| 005 - DATE AND TIME OF LATEST TRANSACTION |
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| control field |
20250625162435.0 |
| 040 ## - CATALOGING SOURCE |
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| Transcribing agency |
CICY |
| 090 ## - LOCALLY ASSIGNED LC-TYPE CALL NUMBER (OCLC); LOCAL CALL NUMBER (RLIN) |
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| Classification number (OCLC) (R) ; Classification number, CALL (RLIN) (NR) |
B-19715 |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION |
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| fixed length control field |
250602s9999 xx |||||s2 |||| ||und|d |
| 245 10 - TITLE STATEMENT |
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| Title |
Determination of Berberine Hydrochloride and Total Glucosides of Paeony by 1H NMR for Quality Control of Fufang Huangliansu Commercial Products |
| 490 0# - SERIES STATEMENT |
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| Volume/sequential designation |
Revista Brasileira de Farmacognosia, 32, p.812-818, 2022 |
| 520 3# - SUMMARY, ETC. |
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| Summary, etc. |
Fufang huangliansu prescription, as a Chinese patent herbal medicine, is widely applied in clinical practice, and its main physiologically active components are berberine hydrochloride and total glucosides of paeony. In this study, a rapid, simple, and accurate quantitative 1H NMR method was developed and validated to determine the two main components of "fufang huangliansu" prescription, berberine hydrochloride and total glucosides of paeony. Dimethyl terephthalate was selected as an internal standard, and the signals for berberine hydrochloride at ? 8.94 ppm (H-13)and total glucosides of paeony at ? 7.55 ppm (H-3?, 5?)were selected for the construction of calibration curves. Method validation was performed in terms of specificity, precision, accuracy, repeatability, stability, and linearity. The results indicated that the assay was precise and in line with the China Food and Drug Administration guidance. The assay has been successfully applied to determine the content of berberine hydrochloride and total glucosides of paeony in "fufang huangliansu" obtained from two pharmaceutical companies. This finding indicates that this 1H NMR method has the potential as a reliable method for quality control of Chinese patent medicines containing berberine. |
| 650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical term or geographic name entry element |
QUANTITATIVE ANALYSIS |
| 650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical term or geographic name entry element |
QNMR |
| 650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical term or geographic name entry element |
METHOD VALIDATION |
| 650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical term or geographic name entry element |
QUALITY EVALUATION |
| 650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical term or geographic name entry element |
TRADITIONAL CHINESE MEDICINE |
| 650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical term or geographic name entry element |
PAEONIA LACTIFLORA |
| 700 12 - ADDED ENTRY--PERSONAL NAME |
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| Personal name |
Zhou, M. |
| 700 12 - ADDED ENTRY--PERSONAL NAME |
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| Personal name |
Yin, S. |
| 700 12 - ADDED ENTRY--PERSONAL NAME |
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| Personal name |
Yu, M. |
| 700 12 - ADDED ENTRY--PERSONAL NAME |
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| Personal name |
Wu, A. |
| 700 12 - ADDED ENTRY--PERSONAL NAME |
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| Personal name |
Wang, C. |
| 700 12 - ADDED ENTRY--PERSONAL NAME |
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| Personal name |
Lu, J. |
| 856 40 - ELECTRONIC LOCATION AND ACCESS |
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| Uniform Resource Identifier |
<a href="https://drive.google.com/file/d/15MRxpxVTjLJ7Cz7UNOEnfLGJv0v31Iu-/view?usp=drivesdk">https://drive.google.com/file/d/15MRxpxVTjLJ7Cz7UNOEnfLGJv0v31Iu-/view?usp=drivesdk</a> |
| Public note |
Para ver el documento ingresa a Google con tu cuenta: @cicy.edu.mx |
| 942 ## - ADDED ENTRY ELEMENTS (KOHA) |
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| Source of classification or shelving scheme |
Clasificación local |
| Koha item type |
Documentos solicitados |
