GC-MS method for characterization and quantification of sitostanol oxidation products (Record no. 54899)

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fixed length control field 01846nam a2200265Ia 4500
003 - CONTROL NUMBER IDENTIFIER
control field MX-MdCICY
005 - DATE AND TIME OF LATEST TRANSACTION
control field 20250625162456.0
040 ## - CATALOGING SOURCE
Transcribing agency CICY
090 ## - LOCALLY ASSIGNED LC-TYPE CALL NUMBER (OCLC); LOCAL CALL NUMBER (RLIN)
Classification number (OCLC) (R) ; Classification number, CALL (RLIN) (NR) B-20819
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245 10 - TITLE STATEMENT
Title GC-MS method for characterization and quantification of sitostanol oxidation products
490 0# - SERIES STATEMENT
Volume/sequential designation ournal of the American Oil Chemists' Society, 81(2), p.135-141, 2004
520 3# - SUMMARY, ETC.
Summary, etc. A new GC-MS method for characterization and quantification of phytosterol oxidation products was developed. Applicability of this method was tested by characterizing sitostanol oxides formed in bulk and then quantifying selected oxides in purified rapeseed oil and tripalmitin matrices in which the complex matrix made oxide analysis difficult. In bulk, nine different sitostanol oxides were characterized, including epimers of 7- and 15-hydroxysitostanol and 6- and 7-ketositostanol. In both lipid matrices, the amounts of sitostanol oxides generated in thermo-oxidation were very low. According to statistical analyses, depending on the oxide, the GC-MS results were the same or slightly higher than those quantified by the more common GC-FID method. Thus, GC-MS provides a powerful alternative for characterization and quantification of phytostanol oxides found in low amounts in complex matrices and is a promising method for future phytosterol oxide studies.
650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element GC-MS QUANTIFICATION
650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element OXIDATIVE STABILITY
650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element PHYTOSTEROL OXIDES
650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element SITOSTANOL
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Soupas, L.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Juntunen, L.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Säynäjoki, S.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Lampi, A. M.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Piironen, V.
856 40 - ELECTRONIC LOCATION AND ACCESS
Uniform Resource Identifier <a href="https://drive.google.com/file/d/13uwTwwk584FxPSvns1_t9I0AgHuTxhil/view?usp=drivesdk">https://drive.google.com/file/d/13uwTwwk584FxPSvns1_t9I0AgHuTxhil/view?usp=drivesdk</a>
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Source of classification or shelving scheme Clasificación local
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  Clasificación local     Ref1 CICY CICY Documento préstamo interbibliotecario 25.06.2025   B-20819 25.06.2025 25.06.2025 Documentos solicitados