Effect of surface modification of graphene oxide with a reactive silane coupling agent on the mechanical properties and biocompatibility of acrylic bone cements (Record no. 55069)

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fixed length control field 02816nam a2200301Ia 4500
003 - CONTROL NUMBER IDENTIFIER
control field MX-MdCICY
005 - DATE AND TIME OF LATEST TRANSACTION
control field 20250625162459.0
040 ## - CATALOGING SOURCE
Transcribing agency CICY
090 ## - LOCALLY ASSIGNED LC-TYPE CALL NUMBER (OCLC); LOCAL CALL NUMBER (RLIN)
Classification number (OCLC) (R) ; Classification number, CALL (RLIN) (NR) B-20990
008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION
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245 10 - TITLE STATEMENT
Title Effect of surface modification of graphene oxide with a reactive silane coupling agent on the mechanical properties and biocompatibility of acrylic bone cements
490 0# - SERIES STATEMENT
Volume/sequential designation Journal of BioMaterials Science, Polymer Edition, 35(3), p.345-363, 2024
520 3# - SUMMARY, ETC.
Summary, etc. Carbon allotrope materials (i.e. carbon nanotubes (CNTs), graphene, graphene oxide (GO)), have been used to reinforce acrylic bone cement. Nevertheless, the intrinsic incompatibility among the above materials produces a deficient interphase. Thus, in this work, the effect of the content of functionalized graphene oxide with a reactive silane on the mechanical properties and cell adhesion of acrylic bone cement was studied. GO was obtained by an oxidative process on natural graphite; subsequently, GO was functionalized with 3-methacryloxypropyltrimethoxysilane (MPS)to enhance the interphase between the graphenic material and acrylic polymeric matrix. Pristine GO and functionalized graphene oxide (GO-MPS)were characterized physicochemically (XPS, XRD, FTIR, and Raman)and morphologically (SEM and TEM). Silanized GO was added into the acrylic bone cement at different concentrations; the resulting materials were characterized mechanically, and their biocompatibility was also evaluated. The physicochemical characterization results showed that graphite was successfully oxidized, and the obtained GO was successfully functionalized with the silane coupling agent (MPS). SEM and TEM images showed that the GO is composed of few stacked layers. Compression testing results indicated a tendency of increasing stiffness and toughness of the acrylic bone cements at low concentration of functionalized GO. Additionally, the bending testing results showed a slightly increase in bone cement strain with the incorporation of GO-MPS. Finally, all samples exhibited cell viability higher than 70 percent, which means that materials are considered non-cytotoxic, according to the ISO 10993-5 standard.
650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element GRAPHENE OXIDE
650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element ACRYLIC BONE CEMENT
650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element SILANE FUNCTIONALIZATION
650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element MECHANICAL PROPERTIES
650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element CELL VIABILITY
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Ayora-Gutiérrez, G.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Abreu-Rejón, A. D.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name May-Pat, A.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Guerrero-Bermea, C.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Fernández-Escamilla, V. V.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Rodríguez-Fuentes, N.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Uribe-Calderon, J. A.
856 40 - ELECTRONIC LOCATION AND ACCESS
Uniform Resource Identifier <a href="https://drive.google.com/file/d/1cNixr0EwfUIm_TXwglv6o0Pv-ZaJe0GT/view?usp=drivesdk">https://drive.google.com/file/d/1cNixr0EwfUIm_TXwglv6o0Pv-ZaJe0GT/view?usp=drivesdk</a>
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Source of classification or shelving scheme Clasificación local
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  Clasificación local     Ref1 CICY CICY Documento préstamo interbibliotecario 25.06.2025   B-20990 25.06.2025 25.06.2025 Documentos solicitados