Unequivocal NMR assignments: O -methoxymethyl esters derivatives of acid chromanones from Calophyllum brasiliense CAMB. (Guanandi) (Record no. 55821)

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fixed length control field 01588nam a2200265Ia 4500
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control field MX-MdCICY
005 - DATE AND TIME OF LATEST TRANSACTION
control field 20250626090917.0
040 ## - CATALOGING SOURCE
Transcribing agency CICY
090 ## - LOCALLY ASSIGNED LC-TYPE CALL NUMBER (OCLC); LOCAL CALL NUMBER (RLIN)
Classification number (OCLC) (R) ; Classification number, CALL (RLIN) (NR) B-21759
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245 10 - TITLE STATEMENT
Title Unequivocal NMR assignments: O -methoxymethyl esters derivatives of acid chromanones from Calophyllum brasiliense CAMB. (Guanandi)
490 0# - SERIES STATEMENT
Series statement Natural Products Research, 22(10), 846-853, 2008
500 ## - GENERAL NOTE
General note Artículo
520 3# - SUMMARY, ETC.
Summary, etc. The present work describes the fractionation of the crude hexane extract (EBHEX) from Calophyllum brasiliense (Clusiaceae) stem bark. Derivatization of DCM2-9 fraction with diazomethane afforded the chromanones inophylloidic acid, isobrasiliensic acid, as well as, a mixture containing isobrasiliensic and brasiliensic acids, in the form of their more stable O-methoxy-methyl esters derivatives 1, 2, and 3, respectively. The isolation of 1 from C. brasiliense is described for the first time herein. The use of two-dimensional NMR methods ( 1 H-COSY, HMQC, and HMBC) allowed the precise determination of 13C and 1 H chemical shifts of compounds 1, 2, and 3.
650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element CALOPHYLLUM BRASILIENSE
650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element ACID CHROMONONES
650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM
Topical term or geographic name entry element UNEQUIVOCAL NMR ASSIGNMENTS
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Caneppele, D.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Vieira, P. C.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Dall'Oglio, E. L.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Da Silva, L. E.
700 12 - ADDED ENTRY--PERSONAL NAME
Personal name Sousa Jr, P. T.
856 40 - ELECTRONIC LOCATION AND ACCESS
Uniform Resource Identifier <a href="https://drive.google.com/file/d/1bGWyN0lGXm5OkAtnMMC0VoYX3jWPq1_c/view?usp=drive_link">https://drive.google.com/file/d/1bGWyN0lGXm5OkAtnMMC0VoYX3jWPq1_c/view?usp=drive_link</a>
Public note Para ver el documento ingresa a Google con tu cuenta: @cicy.edu.mx
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Source of classification or shelving scheme Clasificación local
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  Clasificación local     Ref1 CICY CICY Documento préstamo interbibliotecario 26.06.2025   B-21759 26.06.2025 26.06.2025 Documentos solicitados