MARC details
| 000 -LEADER |
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| fixed length control field |
05108nam a2200289Ia 4500 |
| 001 - CONTROL NUMBER |
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| control field |
000008024 |
| 003 - CONTROL NUMBER IDENTIFIER |
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| control field |
MX-MdCICY |
| 005 - DATE AND TIME OF LATEST TRANSACTION |
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| control field |
20260113131711.0 |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION |
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| fixed length control field |
100715s2011 ne a f p 001 0 eng d |
| 020 ## - INTERNATIONAL STANDARD BOOK NUMBER |
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| International Standard Book Number |
9780123736284 |
| 040 ## - CATALOGING SOURCE |
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| Transcribing agency |
CICY |
| 082 04 - DEWEY DECIMAL CLASSIFICATION NUMBER |
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| Classification number |
543.85 |
| Item number |
S63 2011 |
| 100 1# - MAIN ENTRY--PERSONAL NAME |
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| Personal name |
Sparkman, O. David |
| Dates associated with a name |
1942- |
| 245 10 - TITLE STATEMENT |
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| Title |
Gas chromatography and mass spectrometry : |
| Remainder of title |
a practical guide / |
| Statement of responsibility, etc. |
O David Sparkman, Zelda Penton, Fulton G. Kitson |
| 250 ## - EDITION STATEMENT |
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| Edition statement |
2 ed. |
| 264 31 - PRODUCTION, PUBLICATION, DISTRIBUTION, MANUFACTURE, AND COPYRIGHT NOTICE |
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| Place of production, publication, distribution, manufacture |
Boston, MA : |
| Name of producer, publisher, distributor, manufacturer |
Elsevier, |
| Date of production, publication, distribution, manufacture, or copyright notice |
2011 |
| 300 ## - PHYSICAL DESCRIPTION |
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| Extent |
xix, 611 p. : |
| Other physical details |
il. ; |
| Dimensions |
23 cm. |
| 500 ## - GENERAL NOTE |
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| General note |
Incluye referencias bibliográficas e índice |
| 505 0# - FORMATTED CONTENTS NOTE |
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| Formatted contents note |
Contenido: The fundamentals of GC/MS -- Introduction and history -- Gas chromatography -- The gc/ms interface -- Mass spectrometry instrumentation -- Mass spectral data interpretation -- Quantitation with GC/MS -- GC conditions, derivatization, and mass spectral interpretation -- Of specific compound types -- Acids -- Alcohols -- Aldehydes -- Amides -- Amines -- Amino acid -- Common contaminants -- Drugs and their metabolites -- Esters -- Ethers -- Fluorinated compounds -- Gases -- Glycols -- Halogenated compounds (other than fluorinated) -- Hydrocarbons -- Isocyanates -- Ketones -- Nitriles -- Nitroaromatics -- Nitrogen-containing heterocyclics -- Nucleosides (TMS derivatives) -- Pesticides -- Phenols -- Phosphorus compounds -- Plasticizers and other polymer additives (including phthalates) -- Prostaglandins (MO-TMS derivatives) -- Solvents and their impurities -- Steroids -- Sugars (monosaccharides) -- Sulfur compounds -- Appendices -- A definitions of terms related to gas chromatography -- B definitions of terms related to mass spectrometry -- C atomic masses and isotope abundances -- X+1 and x+2 values for ions containing atoms of C and H based on -- Isotope contributions -- E isotope peak patterns for ions containing atoms of Cl and/or Br -- F steps to follow in the determination of an elemental composition -- Based on isotope peak intensity ratios -- G derivatization in GC/MS -- H points of comparison of LC/MS vs GC/MS -- I list of available EI mass spectral databases -- J information required for reporting a GC/MS analysis -- K third-party software for use with GC/MS -- GC installation and maintenance -- Troubleshooting common GC problems -- N maintenance, operating tips, and troubleshooting for mass spectrometers -- O mixtures for determining mass spectral resolution -- P cross-index chart for GC stationary phases -- Q ions for determining unknown structures. |
| 520 3# - SUMMARY, ETC. |
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| Summary, etc. |
The second edition of Gas Chromatography and Mass Spectrometry: A Practical Guide follows the highly successful first edition by F.G. Kitson, B.S. Larsen, and C.N. McEwen (1996), which was designed as an indispensible resource for GC/MS practitioners regardless of whether they are a novice or well experienced. The Fundamentals section has been extensively reworked from the original edition to give more depth of an understanding of the techniques and science involved with GC/MS. Even with this expansion, the original brevity and simple didactic style has been retained. Information on chromatographic peak deconvolution has been added along with a more in-depth understanding of the use of mass spectral databases in the identification of unknowns. Since the last edition, a number of advances in GC inlet systems and sample introduction techniques have occurred, and they are included in the new edition. Other updates include a discussion on fast GC and options for combining GC detectors with mass spectrometry. The section regarding GC Conditions, Derivatization, and Mass Spectral Interpretation of Specific Compound Types has the same number of compound types as the original edition, but the information in each section has been expanded to not only explain some of the spectra but to also explain why certain fragmentations take place. The number of Appendices has been increased from 12 to 17. The Appendix on Atomic Masses and Isotope Abundances has been expanded to provide tools to aid in determination of elemental composition from isotope peak intensity ratios. An appendix with examples on "Steps to follow in the determination of elemental compositions based on isotope peak intensities" has been added. Appendices on whether to use GC/MS or LC/MS, third-party software for use in data analysis, list of information required in reporting GC/MS data, X+1 and X+2 peak relative intensities based on the number of atoms of carbon in an ion, and list of available EI mass spectral databases have been added. Others such as the ones on derivatization, isotope peak patterns for ions with Cl and/or Br, terms used in GC and in mass spectrometry, and tips on setting up, maintaining and troubleshooting a GC/MS system have all been expanded and updated. |
| 650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical term or geographic name entry element |
CROMATOGRAFIA DE GASES |
| 650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical term or geographic name entry element |
ESPECTROSCOPIA DE MASAS |
| 700 12 - ADDED ENTRY--PERSONAL NAME |
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| Personal name |
Kitson, Fulton G., |
| Relator term |
coaut. |
| 700 12 - ADDED ENTRY--PERSONAL NAME |
|---|
| Personal name |
Penton, Zelda, |
| Relator term |
coaut. |
| 856 40 - ELECTRONIC LOCATION AND ACCESS |
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| Uniform Resource Identifier |
<a href="https://www.cicy.mx/sitios/sib/doctoelectronico/8024.pdf">https://www.cicy.mx/sitios/sib/doctoelectronico/8024.pdf</a> |
| Public note |
Ver tabla de contenido y/o resumen |
| 942 ## - ADDED ENTRY ELEMENTS (KOHA) |
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| Source of classification or shelving scheme |
Dewey Decimal Classification |
| Koha item type |
Libros impresos |
