A Fast and Convenient Procedure for the Acetylation of Alcohols - Synthetic Communication, 34, p.4591-4595, 2004 .

Treatment of different steroidal and aliphatic alcohols with BF3 . OEt2 and acetic anhydride for 5 seconds produced complete acetylation in high to quantitative yields.


O-ACETYLATION
BF3
OET2