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Optimised NMR detection of 13C-2H double labelling in small molecules

Tipo de material: TextoTextoSeries ; Comptes Rendus Chimie, 9(3-4), p.514-519, 2006Trabajos contenidos:
  • Trixie Ann Bartholomeusz
  • François Mesnard
  • François-Xavier Felpin
  • Jacques Lebreton
  • Richard J. Robins
  • Albrecht Roscher
Tema(s): Recursos en línea: Resumen: [13C2H3-methyl]-nicotine was used to optimise the selective NMR detection of the double 13C-2H label with a view towards subsequent metabolism studies. It is concluded that the INEPT transfer from 2H to 13C offers the best choice with regards to sensitivity, resolution and generality for different types of doubly labelled molecules. The necessary experimental arrangements are described.
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[13C2H3-methyl]-nicotine was used to optimise the selective NMR detection of the double 13C-2H label with a view towards subsequent metabolism studies. It is concluded that the INEPT transfer from 2H to 13C offers the best choice with regards to sensitivity, resolution and generality for different types of doubly labelled molecules. The necessary experimental arrangements are described.

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