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090			_aB-9823
245	1	0	_aApplication of acetate derivatives for gas chromatography-mass spectrometry: Novel approaches on carbohydrates, lipids and amino acids analysis
490	0		_vJournal of Chromatography A, 1208(1-2), p.215-222, 2008
520	3		_aThe structure of glycoconjugates has been determined by several chromatographic methods, however gas chromatography-mass spectrometry (GC-MS)has been widely used to identify and quantify the volatile trimethylsilyl and fluoroacyl derivatives. Adapting the reduction/acetylation strategies, we had performed the derivatization of all monosaccharide class, as well as amino acids and OH-fatty acids as fromdifferent glycoconjugates. Uronic acids gave characteristic ions atm/z 143, 156 and 173, and 19 amino acids derivatives, gave molecular ions [M]+ and daughter ions of [M-59]+ and [M-43]+ on electron impact (EI)-MS, which provide their rapid identification
650	1	4	_aALDITOL-ACETATE-METHYL-ESTERS
650	1	4	_aACETATE-METHYL-ESTERS
650	1	4	_aURONIC ACIDS
650	1	4	_aAMINO ACIDS
650	1	4	_aLIPIDS
650	1	4	_aGC-MS
700	1	2	_aSassaki, G.L.
700	1	2	_aSouza, L.M.
700	1	2	_aSerrato, R.V.
700	1	2	_aCipriani, T.R.
700	1	2	_aGorin, P.A.J.
700	1	2	_aIacomini, M.
856	4	0	_uhttps://drive.google.com/file/d/1WS4yDG3kebK29QabF94jg-GleUu0bPAQ/view?usp=drivesdk _zPara ver el documento ingresa a Google con tu cuenta: @cicy.edu.mx
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