000 01997nam a2200265Ia 4500
003 MX-MdCICY
005 20250625162412.0
040 _cCICY
090 _aB-18429
245 1 0 _aCharacterisation of halloysite by spectroscopy.
490 0 _vIn Developments in Clay Science. Elsevier., 7, p.115-136)., 2016
520 3 _aThis chapter provides an overview of results obtained by a variety of spectroscopic techniques. The most common techniques employed are infrared (IR)and Raman spectroscopy, which enable detailed observation of the behaviour of water and OH-groups and the type of H-bonds formed. The inner-surface OH-groups that normally form H-bonds with adjacent layers in the kaolins and form H-bonds with water in the interlayer in halloysite. Infrared emission spectroscopy showed that the four inner and inner-surface OH-groups were removed at different temperatures, at different rates, or both. A slight increase in the Al 2p binding energy observed in the spectra of X-ray photoelectron spectroscopy from kaolinite to halloysite reflects a change in the stacking order due to the interlayer water. The overall shape of the O 1s is indicative of two peaks associated with the oxygen atoms and with the OH-groups. A third, very weak peak was observed to be associated with interlayer water that is still present despite the ultrahigh vacuum.
650 1 4 _aHALLOYSITE
650 1 4 _aKAOLININFRARED SPECTROSCOPY
650 1 4 _aRAMAN SPECTROSCOPY
650 1 4 _aX-RAY PHOTOELECTRON SPECTROSCOPY
650 1 4 _aSOLID-STATE MAGIC-ANGLE-SPINNING NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY
650 1 4 _aELECTRON SPIN RESONANCE SPECTROSCOPY
650 1 4 _aMÖSSBAUER SPECTROSCOPY
650 1 4 _aCATHODELUMINESCENCE
700 1 2 _aKloprogge, J. T.
856 4 0 _uhttps://drive.google.com/file/d/1kgovnzB8hajhTlztKb9K4AgrXGdR8GFE/view?usp=drivesdk
_zPara ver el documento ingresa a Google con tu cuenta: @cicy.edu.mx
942 _2Loc
_cREF1
008 250602s9999 xx |||||s2 |||| ||und|d
999 _c52581
_d52581