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245 1 0 _aFT-IR study for hydroxyapatite/collagen nanocomposite cross-linked by glutaraldehyde
490 0 _vBioMaterials, 23(24), p.4811-4818, 2002
520 3 _aFT-IR analysis was performed for the hydroxyapatite (HAp)/collagen (COL)nanocomposite cross-linked by glutaraldehyde (GA). The amide bands I, II and III from COL matrix, and phosphate and carbonate bands from HAp were identified. The amide B band arising from C-H stretching mode showed a sensitive conformation by the degree of cross-linking. The amide I band showed a complicate conformational change by the degree of cross-linking. The characteristic amide I band at 1685 cm?1, which is known as an aging parameter in the biological bone, did not show a monotonous tendency by the degree of cross-linking. The relative contents of the organics in the cross-linked HAp/COL nanocomposite were evaluated as an integration ratio between the amide I band at 1600-1700 cm?1 and PO43? band at 900-1200 cm?1. The increase of the organics content by the cross-linking is enabled by the further organization of Ca2+ ions of HAp crystals in HAp/COL nanocomposite. The complicate conformational behavior in the amide I, II and III bands seems to be affected by the cross-linking induced directional arrangement of HAp/COL nanocomposite fibrils.
650 1 4 _aHYDROXYAPATITE
650 1 4 _aCOLLAGEN
650 1 4 _aCROSS-LINKING
650 1 4 _aGLUTARALDEHYDE
650 1 4 _aFT-IR
700 1 2 _aChang, M. C.
700 1 2 _aTanaka, J.
856 4 0 _uhttps://drive.google.com/file/d/1ytnxh61dcUNVfbMQDUC-VXAKEEI1oEPs/view?usp=drivesdk
_zPara ver el documento ingresa a Google con tu cuenta: @cicy.edu.mx
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