Apolar chromatography on Sephadex LH-20 combined with high-speed counter-current chromatography High yield strategy for structurally closely related analytes-Destruxin derivatives from Metarhizium anisopliae as a case study (Record no. 44009)
[ view plain ]
| 000 -LEADER | |
|---|---|
| fixed length control field | 01559nam a2200277Ia 4500 |
| 003 - CONTROL NUMBER IDENTIFIER | |
| control field | MX-MdCICY |
| 005 - DATE AND TIME OF LATEST TRANSACTION | |
| control field | 20250625140619.0 |
| 040 ## - CATALOGING SOURCE | |
| Transcribing agency | CICY |
| 090 ## - LOCALLY ASSIGNED LC-TYPE CALL NUMBER (OCLC); LOCAL CALL NUMBER (RLIN) | |
| Classification number (OCLC) (R) ; Classification number, CALL (RLIN) (NR) | B-9763 |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION | |
| fixed length control field | 250602s9999 xx |||||s2 |||| ||und|d |
| 245 10 - TITLE STATEMENT | |
| Title | Apolar chromatography on Sephadex LH-20 combined with high-speed counter-current chromatography High yield strategy for structurally closely related analytes-Destruxin derivatives from Metarhizium anisopliae as a case study |
| 490 0# - SERIES STATEMENT | |
| Volume/sequential designation | Journal of Chromatography A, 1117(1), p.67-73, 2006 |
| 520 3# - SUMMARY, ETC. | |
| Summary, etc. | A novel high yield isolation procedure for lipophilic cyclic peptide derivatives is presented. Destruxin (dtx)A, B, D, E, and E-diol retrieval from Metarhizium anisopliae culture broth was achieved with a three-step purification protocol. After liquid-liquid extraction column chromatography over Sephadex LH-20 served as enrichment step. High-speed counter-current chromatography (HSCCC)was used for the final purification.Within the first chromatographic step dtx D and dtx E-diol were separated in purities exceeding 90 |
| 650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM | |
| Topical term or geographic name entry element | METARHIZIUM ANISOPLIAE |
| 650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM | |
| Topical term or geographic name entry element | DESTRUXINS |
| 650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM | |
| Topical term or geographic name entry element | SEPHADEX-LH20 |
| 650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM | |
| Topical term or geographic name entry element | HSCCC |
| 650 14 - SUBJECT ADDED ENTRY--TOPICAL TERM | |
| Topical term or geographic name entry element | HIGH-SPEED COUNTER-CURRENT CHROMATOGRAPHY |
| 700 12 - ADDED ENTRY--PERSONAL NAME | |
| Personal name | Seger, C. |
| 700 12 - ADDED ENTRY--PERSONAL NAME | |
| Personal name | Eberhart, K. |
| 700 12 - ADDED ENTRY--PERSONAL NAME | |
| Personal name | Sturm, S. |
| 700 12 - ADDED ENTRY--PERSONAL NAME | |
| Personal name | Strasser, H. |
| 700 12 - ADDED ENTRY--PERSONAL NAME | |
| Personal name | Stuppner, H. |
| 856 40 - ELECTRONIC LOCATION AND ACCESS | |
| Uniform Resource Identifier | <a href="https://drive.google.com/file/d/1kS_2wsFNxA-aSBntOAfZ2BlVnGmu5BbH/view?usp=drivesdk">https://drive.google.com/file/d/1kS_2wsFNxA-aSBntOAfZ2BlVnGmu5BbH/view?usp=drivesdk</a> |
| Public note | Para ver el documento ingresa a Google con tu cuenta: @cicy.edu.mx |
| 942 ## - ADDED ENTRY ELEMENTS (KOHA) | |
| Source of classification or shelving scheme | Clasificación local |
| Koha item type | Documentos solicitados |
| Lost status | Source of classification or shelving scheme | Damaged status | Not for loan | Collection | Home library | Current library | Shelving location | Date acquired | Total checkouts | Full call number | Date last seen | Price effective from | Koha item type |
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| Clasificación local | Ref1 | CICY | CICY | Documento préstamo interbibliotecario | 25.06.2025 | B-9763 | 25.06.2025 | 25.06.2025 | Documentos solicitados |