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Omphalotin, A New Cyclic Peptide with Potent Nematicidal Activity from Omphalotus Olearius II. Isolation and Structure Determination

Tipo de material: TextoTextoSeries ; Natural Product Letters, 10(1), p.33-38, 1997Trabajos contenidos:
  • Sterner, O
  • Etzel, W
  • Mayer, A
  • Anke, H
Tema(s): Recursos en línea: Resumen: The structure of the potent nematicide omphalotin, isolated from the mycelia of the basidiomycete Omphalotus olearius, was determined by spectroscopic techniques. Omphalotin is a cyclic dodecapeptide consisting of 3 glycine, 5 valine, 3 isoleucine and 1 tryptophane, and 9 of the 12 a-nitrogens are methylated. HMBC and NOESY correlations between the N-methyl groups and the a-carbonda-hydrogens established the sequence of amino acids.
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The structure of the potent nematicide omphalotin, isolated from the mycelia of the basidiomycete Omphalotus olearius, was determined by spectroscopic techniques. Omphalotin is a cyclic dodecapeptide consisting of 3 glycine, 5 valine, 3 isoleucine and 1 tryptophane, and 9 of the 12 a-nitrogens are methylated. HMBC and NOESY correlations between the N-methyl groups and the a-carbonda-hydrogens established the sequence of amino acids.

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